A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions

Science Communicator Platform

Stay connected! Follow us on X network (Twitter):

Share By

A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions Publisher

Mouradzadegun A^{1, 2} ; Mostafavi MA¹ ; Ganjali MR^{2, 3}

Source: Reaction Kinetics# Mechanisms and Catalysis Published:2018

Abstract

N-propyl sulfamic acid supported nano-catalyst on the basis of calix[4]resorcinarene was prepared via the efficient and facile reaction of amine functionalized polycalix[4]resorcinarene with chlorosulfonic acid. The achieved catalytic system was characterized using some spectroscopic techniques such as Fourier transform Infrared (FT-IR) spectroscopy, field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), and CHNS elemental analysis. This newly developed acidic catalyst was employed efficiently in a one-pot three-component condensation reaction of aromatic aldehydes, dimedone and phthalhydrazide for the synthesis of 2H-indazolo[2,1-b]phthalazine-trione derivatives through an easy and eco-friendly methodology. The catalyst was easily separated from the reaction mixture by simple filtration and the desired products were achieved in good to excellent yields in short reaction times. © 2018, Akademiai Kiado, Budapest, Hungary.

Related Docs

View other Related Docs

1. Sulfamic Acid Functionalized 3D-Network Nanoporous Polymer Based on Calix[4]Resorcinarene: A Recyclable Heterogeneous Nanocatalyst for the Efficient Synthesis of 14-Aryl-14H-Dibenzo[A,J]Xanthenes Under Thermal Neat Conditions, Journal of Inclusion Phenomena and Macrocyclic Chemistry (2018)

2. High Nitrogen-Doped Porous Carbon Material From Porous Aromatic Framework; an Approach to Bi-Functional Metal-Free Electrocatalyst, Inorganic Chemistry Communications (2024)

3. A Reactive and Environmentally Friendly Protocol for Expeditious Synthesis of Various Resorcinarenes Using Zinc Hydrogen Sulfate, Supramolecular Chemistry (2019)

Experts (# of related papers)

Mohammad Mahdavi (3)

Mehdi Khoobi (1)

Other Related Docs

4. A Facile and Green Synthesis of 2,4,6-Triarylpyridine Derivatives Using the Modified Mesoporous Organic Polymer Based on Calix [4]Resorcinarene: As an Efficient and Reusable Heterogeneous Acidic Catalyst, Kinetics and Catalysis (2019)

5. Synthesis and Characterization of Γ-Fe2o3@Sio2-(Ch2)3-Pdtc-Pd Magnetic Nanoparticles: A New and Highly Active Catalyst for the Heck/Sonogashira Coupling Reactions, New Journal of Chemistry (2019)

6. The Synthesis of 2,3-Dihydroquinazoline-4(1H)-One and Dihydroisoindolo[2,1-A]Quinazoline-5,11-Dione Derivatives in the Presence of Imidazolium Ionic Liquid Sulfonic Acid Functionalized Sba-15: A Novel Feature of Sba-15, Arkivoc (2018)

7. Copper Supported Imidazolylpyridine Modified Spion As an Efficient Catalyst for Eco-Friendly, One-Pot and Green Synthesis of Novel (3-Cyanothiophen-2-Yl)-N-(Arylsulfonyl)Acetimidamide Derivatives, Current Organic Synthesis (2023)

8. Rapid and Green Synthesis of 4H-Benzo[B]Pyrans Using Triethanolamine As an Efficient Homogeneous Catalyst Under Ambient Conditions, Research on Chemical Intermediates (2020)

Style	Citing Format
MLA	Mouradzadegun A, Mostafavi MA, Ganjali MR. "A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions." Reaction Kinetics# Mechanisms and Catalysis, vol. 124, no. 2, 2018, pp. 741-755.
APA	Mouradzadegun A, Mostafavi MA, Ganjali MR (2018). A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions. Reaction Kinetics# Mechanisms and Catalysis, 124(2), 741-755.
Chicago	Mouradzadegun A, Mostafavi MA, Ganjali MR. "A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions." Reaction Kinetics# Mechanisms and Catalysis 124, no. 2 (2018): 741-755.
Harvard	Mouradzadegun A, Mostafavi MA, Ganjali MR (2018) 'A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions', Reaction Kinetics# Mechanisms and Catalysis, 124(2), pp. 741-755.
Vancouver	Mouradzadegun A, Mostafavi MA, Ganjali MR. A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions. Reaction Kinetics# Mechanisms and Catalysis. 2018;124(2):741-755.
BibTex	@article{ author = {Mouradzadegun A and Mostafavi MA and Ganjali MR}, title = {A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions}, journal = {Reaction Kinetics# Mechanisms and Catalysis}, volume = {124}, number = {2}, pages = {741-755}, year = {2018} }
RIS	TY - JOUR AU - Mouradzadegun A AU - Mostafavi MA AU - Ganjali MR TI - A Novel Sulfamic Acid Functionalized Nano-Catalyst on the Basis of Calix[4]Resorcinarene for the Green One-Pot Synthesis of 2H-Indazolo[2,1-B]Phthalazine-Triones Under Thermal Solvent-Free Conditions JO - Reaction Kinetics# Mechanisms and Catalysis VL - 124 IS - 2 SP - 741 EP - 755 PY - 2018 ER -

Science Communicator Platform

Authors

Abstract